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Incredibly electrophilic keteniminium ions generated in situ were employed as powerful intermediates for cascade [1,5]-hydride transfer/cyclization, via which inert benzylic and non-benzylic C(sp3)–H bonds without a directing group were directly functionalized to furnish complex polycycles in a single operation.

Graphical abstract: Direct functionalization of benzylic and non-benzylic C(sp3)–H bonds via keteniminium ion initiated cascade [1,5]-hydrogen transfer/cyclization

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