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Alkaline hydrolysis of RTeBr3 (R = 2-phenylazophenyl) gave intramolecularly stabilized homometallic, heptanuclear organotellurium oxide cluster R6Te7O11 (4) in good yield.

Graphical abstract: Hydrolysis of 2-phenylazophenyltellurium trihalides: isolation of an unprecedented homometallic, discrete heptanuclear organotellurium oxide cluster

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