Solid-state and solution phase metathetical synthesis of copper indium chalcogenides

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Claire J. Carmalt, Daniel E. Morrison and Ivan P. Parkin


Abstract

Copper indium chalcogenides, of the type CuInE2 (E=S, Se and Te), have been successfully prepared by solid-state and solution phase metathetical reactions of CuBr or CuCl2 , InCl3 and the appropriate sodium chalcogenide (Na2E). The copper indium chalcogenides were analysed by powder X-ray diffraction, scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDXA) and FTIR spectroscopy.


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