Size matters: altering the metal-surface coordination in micropores via structural confinement effects

Scott A. Southern, Austin Thompson, Aaron D. Sadow and Frédéric A. Perras

Inorg. Chem. Front., 2024, 11, 6862
DOI: 10.1039/D4QI01261E

Observing the three-dimensional dynamics of supported metal complexes

Alexander L. Paterson, Da-Jiang Liu, Uddhav Kanbur, Aaron D. Sadow and Frédéric A. Perras

Inorg. Chem. Front., 2021, 8, 1416
DOI: 10.1039/D0QI01241F

Accurate heteronuclear distance measurements at all magic-angle spinning frequencies in solid-state NMR spectroscopy

Lixin Liang, Yi Ji, Zhenchao Zhao, Caitlin M. Quinn, Xiuwen Han, Xinhe Bao, Tatyana Polenova and Guangjin Hou

Chem. Sci., 2021, 12, 11554
DOI: 10.1039/D1SC03194E

1H chemical shift anisotropy: a high sensitivity solid-state NMR dynamics probe for surface studies?

Scott A. Southern, Da-Jiang Liu, Puranjan Chatterjee, Yuting Li and Frédéric A. Perras

Phys. Chem. Chem. Phys., 2023, 25, 5348
DOI: 10.1039/D2CP04406D

2H–13C correlation solid-state NMR for investigating dynamics and water accessibilities of proteins and carbohydrates

Martin D. Gelenter, Tuo Wang, Shu-Yu Liao, Hugh O’Neill and Mei Hong

J Biomol NMR, 2017, 68, 257
DOI: 10.1007/s10858-017-0124-7

Supercycled R-symmetry sequences for robust heteronuclear polarization transfer in solid-state NMR

Lixin Liang, Chao Shang, Kuizhi Chen and Guangjin Hou

Journal of Magnetic Resonance, 2022, 344, 107310
DOI: 10.1016/j.jmr.2022.107310

Expanding the horizons for structural analysis of fully protonated protein assemblies by NMR spectroscopy at MAS frequencies above 100 kHz

Jochem Struppe, Caitlin M. Quinn, Manman Lu, Mingzhang Wang, Guangjin Hou, Xingyu Lu, Jodi Kraus, Loren B. Andreas, Jan Stanek, Daniela Lalli, Anne Lesage, Guido Pintacuda, Werner Maas, Angela M. Gronenborn and Tatyana Polenova

Solid State Nuclear Magnetic Resonance, 2017, 87, 117
DOI: 10.1016/j.ssnmr.2017.07.001

Determining the Three-Dimensional Structures of Silica-Supported Metal Complexes from the Ground Up

Frédéric A. Perras, Uddhav Kanbur, Alexander L. Paterson, Puranjan Chatterjee, Igor I. Slowing and Aaron D. Sadow

Inorg. Chem., 2022, 61, 1067
DOI: 10.1021/acs.inorgchem.1c03200

Natural Abundance 17O DNP NMR Provides Precise O−H Distances and Insights into the Brønsted Acidity of Heterogeneous Catalysts

Frédéric A. Perras, Zhuoran Wang, Pranjali Naik, Igor I. Slowing and Marek Pruski

Angewandte Chemie, 2017, 129, 9293
DOI: 10.1002/ange.201704032

Comparative Study of REDOR and CPPI Derived Order Parameters by 1H-Detected MAS NMR and MD Simulations

Sam Asami and Bernd Reif

J. Phys. Chem. B, 2017, 121, 8719
DOI: 10.1021/acs.jpcb.7b06812

Aromatic Ring Dynamics, Thermal Activation, and Transient Conformations of a 468 kDa Enzyme by Specific 1H–13C Labeling and Fast Magic-Angle Spinning NMR

Diego F. Gauto, Pavel Macek, Alessandro Barducci, Hugo Fraga, Audrey Hessel, Tsutomu Terauchi, David Gajan, Yohei Miyanoiri, Jerome Boisbouvier, Roman Lichtenecker, Masatsune Kainosho and Paul Schanda

J. Am. Chem. Soc., 2019, 141, 11183
DOI: 10.1021/jacs.9b04219

Ultrafast Magic Angle Spinning Solid-State NMR Spectroscopy: Advances in Methodology and Applications

Yusuke Nishiyama, Guangjin Hou, Vipin Agarwal, Yongchao Su and Ayyalusamy Ramamoorthy

Chem. Rev., 2023, 123, 918
DOI: 10.1021/acs.chemrev.2c00197

Time-domain proton-detected local-field NMR for molecular structure determination in complex lipid membranes

Anika Wurl, Kay Saalwächter and Tiago Mendes Ferreira

Magn. Reson., 2023, 4, 115
DOI: 10.5194/mr-4-115-2023

Dynamics in the Intact fd Bacteriophage Revealed by Pseudo 3D REDOR-Based Magic Angle Spinning NMR

Orr Simon Lusky, Dvir Sherer and Amir Goldbourt

JACS Au, 2024, 4, 3619
DOI: 10.1021/jacsau.4c00549

Comparison of methods for the NMR measurement of motionally averaged dipolar couplings

Scott A. Southern and Frédéric A. Perras

Journal of Magnetic Resonance, 2024, 364, 107710
DOI: 10.1016/j.jmr.2024.107710

Proton-detected 15N-1H dipolar coupling/1H chemical shift correlation experiment for the measurement of NH distances in biological solids under fast MAS solid-state NMR

Ekta Nehra, Neelam Sehrawat, Takeshi Kobayashi, Yusuke Nishiyama and Manoj Kumar Pandey

Journal of Magnetic Resonance Open, 2022, 10-11, 100028
DOI: 10.1016/j.jmro.2021.100028

A modification of γ-encoded RN symmetry pulses for increasing the scaling factor and more accurate measurements of the strong heteronuclear dipolar couplings

Evgeny Nimerovsky and Corinne P. Soutar

Journal of Magnetic Resonance, 2020, 319, 106827
DOI: 10.1016/j.jmr.2020.106827

Determination of accurate 19F chemical shift tensors with R-symmetry recoupling at high MAS frequencies (60–100 kHz)

Gal Porat-Dahlerbruch, Jochem Struppe, Caitlin M. Quinn, Angela M. Gronenborn and Tatyana Polenova

Journal of Magnetic Resonance, 2022, 340, 107227
DOI: 10.1016/j.jmr.2022.107227

Recent progress in dipolar recoupling techniques under fast MAS in solid-state NMR spectroscopy

Yi Ji, Lixin Liang, Xinhe Bao and Guangjin Hou

Solid State Nuclear Magnetic Resonance, 2021, 112, 101711
DOI: 10.1016/j.ssnmr.2020.101711

Solid-State NMR: Methods for Biological Solids

Sahil Ahlawat, Kaustubh R. Mote, Nils-Alexander Lakomek and Vipin Agarwal

Chem. Rev., 2022, 122, 9643
DOI: 10.1021/acs.chemrev.1c00852

Natural Abundance 17O DNP NMR Provides Precise O−H Distances and Insights into the Brønsted Acidity of Heterogeneous Catalysts

Frédéric A. Perras, Zhuoran Wang, Pranjali Naik, Igor I. Slowing and Marek Pruski

Angew Chem Int Ed, 2017, 56, 9165
DOI: 10.1002/anie.201704032

Paramagnetic solid-state NMR of proteins

Ming Tang and Dennis Lam

Solid State Nuclear Magnetic Resonance, 2019, 103, 9
DOI: 10.1016/j.ssnmr.2019.101621

Phase-sensitive γ-encoded recoupling of heteronuclear dipolar interactions and 1H chemical shift anisotropy

Frédéric A. Perras, Alexander L. Paterson and Takeshi Kobayashi

Solid State Nuclear Magnetic Resonance, 2021, 111, 101712
DOI: 10.1016/j.ssnmr.2020.101712

Solid-State NMR Dipolar and Chemical Shift Anisotropy Recoupling Techniques for Structural and Dynamical Studies in Biological Systems

Lixin Liang, Yi Ji, Kuizhi Chen, Pan Gao, Zhenchao Zhao and Guangjin Hou

Chem. Rev., 2022, 122, 9880
DOI: 10.1021/acs.chemrev.1c00779

Overcoming Prohibitively Large Radiofrequency Demands for the Measurement of Internuclear Distances with Solid-State NMR under Fast Magic-Angle Spinning

Mukul G. Jain, G. Rajalakshmi, P. K. Madhu, Vipin Agarwal and Kaustubh R. Mote

J. Phys. Chem. B, 2020, 124, 1444
DOI: 10.1021/acs.jpcb.9b11849

Measuring Dipolar Order Parameters in Nondeuterated Proteins Using Solid-State NMR at the Magic-Angle-Spinning Frequency of 100 kHz

Pravin P. Taware, Mukul G. Jain, Sreejith Raran-Kurussi, Vipin Agarwal, P. K. Madhu and Kaustubh R. Mote

J. Phys. Chem. Lett., 2023, 14, 3627
DOI: 10.1021/acs.jpclett.3c00492

Measurement of C–H distances in solids at natural abundance via proton-detected fast MAS NMR spectroscopy

Yayatika Bhardwaj, Ketan Kumar Rohilla, Yusuke Nishiyama and Manoj Kumar Pandey

Solid State Nuclear Magnetic Resonance, 2025, 139, 102031
DOI: 10.1016/j.ssnmr.2025.102031

Evaluating the motional timescales contributing to averaged anisotropic interactions in MAS solid-state NMR

Kathrin Aebischer, Lea Marie Becker, Paul Schanda and Matthias Ernst

Magn. Reson., 2024, 5, 69
DOI: 10.5194/mr-5-69-2024

Simultaneous recoupling of chemical shift tensors of two nuclei by R-symmetry sequences

Gal Porat-Dahlerbruch and Tatyana Polenova

Journal of Magnetic Resonance, 2023, 348, 107382
DOI: 10.1016/j.jmr.2023.107382