Herein, we uncover structural dimensionality as a key factor governing CO₂/C₂H₂ separation in MWW zeolites. Exfoliated MWW monolayers outperform 3D frameworks by extended breakthrough interval with higher selectivity. Combined experimental and DFT analyses reveal site-specific adsorption and reduced transport barriers, establishing dimensionality as a new design axis for molecular sieving.
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A. Li, X. Zhang, Y. Zhang, M. Shamzhy, X. Guo, Y. Wan, B. Li, X. Hu, R. Cai and F. Zhou, Mater. Horiz., 2026, Accepted Manuscript , DOI: 10.1039/D5MH02061A
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