A chiral substance crystallizing as a racemic compound was deracemized using mechanochemistry. The material was engineered as a mixed crystal with a compound crystallizing as a conglomerate. A threefold increase of the yield of deracemization using high-energy milling is observed compared to regular solution process due to improved solid-state miscibility.
C. Pinètre, C. Lopes, C. Brandel, G. Coquerel, T. Leyssens, Y. CARTIGNY and V. Dupray, Chem. Commun., 2026, Accepted Manuscript , DOI: 10.1039/D6CC01337F
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