A millisecond-resolved flash-pulse heating strategy generates densely dispersed CoNiOx nanoclusters on gel-derived carbon. CoNiOx (Ni/Co = 4:1) delivers 88.9% H2O2 selectivity in neutral electrolyte, which is attributed to a maximum H2O2 production rate of 1.40 mol h−1 g−1 in a gas-diffusion flow cell, as supported by regulated *OOH adsorption on Ni-Co-O sites.
S. Lin, X. Liu, Y. Liu, Z. Jin and P. Li, Chem. Commun., 2026, Accepted Manuscript , DOI: 10.1039/D6CC00201C
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