Acidic hydrogen peroxide electrosynthesis faces catalyst instability issues. We develop MIL-125@Ppy catalyst, achieving a high H2O2 electrosynthesis yield rate of 69.5 mol gcat−1 h−1 (Faradaic efficiency of 82.2%) at pH = 1 for more than 50 hrs. Spectroscopic evidence confirms *OOH key mediate stabilization by in situ formed Ti-N bridge sites enables the selective and stable two-electron pathway
Y. Zhang, S. Ding and S. Chen, Chem. Commun., 2026, Accepted Manuscript , DOI: 10.1039/D5CC06247K
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