Iron-catalyzed cascade C–C and C–O bond formation of 2,4-dienals with donor–acceptor cyclopropanes (DACs) has been developed to furnish hexahydrocyclopentapyrans. Optically active DACs can be coupled stereospecifically (>97% ee). Chirality transfer, use of iron-catalysis and substrate scope are the salient practical features.
M. Mishra, K. Verma, S. Banerjee and T. Punniyamurthy, Chem. Commun., 2024, 60, 2788 DOI: 10.1039/D3CC06261A
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