The antibiotic vancomycin and its derivatives CDP-I and aglucovancomycin have been studied by 13C n.m.r. spectroscopy. The spectra have been partially assigned by means of model compounds, pH titrations, addition of lanthanide ions, selective {1H} decoupling, and 13C labelling experiments, allowing all but four of the 66 carbon atoms in vancomycin to be assigned. Full details of the assignment are presented.
A. Bongini, J. Feeney, M. P. Williamson and D. H. Williams, J. Chem. Soc., Perkin Trans. 2, 1981, 201 DOI: 10.1039/P29810000201
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