(R)-(–)-Muscone was synthesized in a stereocontrolled manner via the diastereoselective conjugate addition to a cyclic α,β-unsaturated ester of (R,R)-cyclohexane-1,2-diol accompanied by spontaneous Dieckmann condensation.
T. Ogawa, C. Fang, H. Suemune and K. Sakai, J. Chem. Soc., Chem. Commun., 1991, 1438 DOI: 10.1039/C39910001438
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