A simple and inexpensive procedure for the reductive coupling of nitroarenes to hydrazoarenes with aluminium and potassium hydroxide in methanol at ambient temperature is reported. The coupling is proposed to proceed by single electron transfer from aluminium.
J. M. Khurana and S. Singh, J. Chem. Soc., Perkin Trans. 1, 1999, 1893 DOI: 10.1039/A807194B
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