The reductive carboxyalkylation of electron-rich alkenes by α-halogenoesters in the presence of triphenylsilane under free-radical conditions is catalysed by thiols: prochiral alkenes give optically-active adducts when the thiol catalyst is homochiral.
H. Dang, K. Kim and B. P. Roberts, Chem. Commun., 1998, 1413 DOI: 10.1039/A802826E
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