Issue 8, 1997
From the journal:

Chemical Communications

Oxidation of monomeric N,N′-dilithium N,N′-bis(di-tert-butylmethylsilyl)hydraz ide to the diazene

Henning Witte-Abel,   Uwe Klingebiel  and  Mathias Noltemeyer  

Abstract

The reaction between the bis(silyl)hydrazine RNHNHR and butyllithium in thf affords the first monomeric dilithium bis(silyl)hydrazide RNLiNLiR·3thf 1 (R = SiBu t 2 Me) and the crystal structure of 1 is presented; the thermally stable bis(silyl)diazene RN[double bond, length as m-dash]NR 2 (R = SiBu t 2 Me) is formed in the reaction between 1 and Br 2 .

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Article information

DOI
https://doi.org/10.1039/A700926G
Article type
Paper

Chem. Commun., 1997, 771-772

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Oxidation of monomeric N,N′-dilithium N,N′-bis(di-tert-butylmethylsilyl)hydraz ide to the diazene

H. Witte-Abel, U. Klingebiel and M. Noltemeyer, Chem. Commun., 1997, 771 DOI: 10.1039/A700926G

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