Variable temperature 13C n.m.r. measurements of chemical shift anisotropy in a powdered sample of U(C6H6)Fe(C5H5)]+[AsF′U]–(1) reveal phase transitions between three different crystal forms, each characterised by a different combination of internal ring rotations and external rotations of the whole cation.
I. Sayer, J. Chem. Soc., Chem. Commun., 1988, 227 DOI: 10.1039/C39880000227
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