3H-λ5-Phospholes were synthesized by reaction of alkyldiphenylphosphine imines (1) with dimethyl acetylenedicarboxylate and subsequent treatment of the adduct (2) with potassium hydride.
J. Barluenga, F. López and F. Palacios, J. Chem. Soc., Chem. Commun., 1986, 1574 DOI: 10.1039/C39860001574
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