The α-alkoxycarbonylcycloalkanones (4) were synthesized in 39–79% yields from the (n+3), (n+3)-dichloro-1-trimethylsiloxybicyclo[n.1.0]alkanes (1c; n= 4, 5, and 10) by electrolysis in alcohols in the presence of iron (III) nitrate at –13 to –10 °C.
S. Torii, T. Okamoto and N. Ueno, J. Chem. Soc., Chem. Commun., 1978, 293 DOI: 10.1039/C39780000293
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