Anodic oxidation of the β-oxocarboxylate ethylene acetals (1a—e) in anhydrous methanol gives the 2-methoxy-1,4-dioxans (2a—e) in 40–60% yield.
D. Lelandais, C. Bacquet and J. Einhorn, J. Chem. Soc., Chem. Commun., 1978, 194 DOI: 10.1039/C39780000194
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