In acidic aqueous ethanolic media, at –7 °C, the reversible two-electron cathodic reduction of nitropyridines (PyNO2) leads to the corresponding dihydroxyamines [PyN(OH)2] which produce nitrosopyridines (PyNO) by elimination of water.
A. Darchen and C. Moinet, J. Chem. Soc., Chem. Commun., 1976, 487 DOI: 10.1039/C39760000487
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