The dichlorides of triphenylarsine and triphenylstibine can be prepared in high yield, by the reaction in toluene solution at 0°, between triphenylarsine or triphenylstibine and sulphuryl chloride.
A. J. Banister and L. F. Moore, J. Chem. Soc. A, 1968, 1137 DOI: 10.1039/J19680001137
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