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Volume 173, 2014
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Synthesis of face-centred cubic Cs3C60 in THF

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Abstract

A solution chemistry synthetic route yields Cs3C60 with a face-centred cubic structure. The described method uses well-established Schlenk techniques and THF as a solvent. The controlled addition of an organo-metallic salt reducing agent prevents the formation of C604− salts. The final product can be precipitated from the solution using hexane as an anti-solvent.

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Publication details

The article was received on 30 Apr 2014, accepted on 11 Jul 2014 and first published on 11 Jul 2014


Article type: Paper
DOI: 10.1039/C4FD00085D
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Citation: Faraday Discuss., 2014,173, 95-103

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    Synthesis of face-centred cubic Cs3C60 in THF

    A. G. McLennan, A. Y. Ganin, Y. Takabayashi, R. H. Colman, R. H. Zadik, M. J. Rosseinsky and K. Prassides, Faraday Discuss., 2014, 173, 95
    DOI: 10.1039/C4FD00085D

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