PLATFORM UPDATE:
Attempts to synthesize a phenanthroline palladium(0) complex with an eta2 -coordinated nitrosoarene starting from a palladium(II) precursor and the corresponding aryl hydroxylamine afforded instead apparent palladium(I) metallacyclic complexes that, on a closer inspection, were proven to be Pd(II) complexes with a new kind of radical-anionic nitrosoarene ligand.
D. R. Ramadan, M. A. Fouad, F. Ferretti, A. Brotons-Rufes, P. Macchi, L. Sorace, M. Gimferrer, C. Costabile and F. Ragaini, Dalton Trans., 2026, Accepted Manuscript , DOI: 10.1039/D6DT01038E
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