We developed tridentate rotaxane ligands to stabilise a dynamic Cu(I) centre with an empty coordination site for O2 reduction. Electrocatalytic activity and selectivity can be controlled by the interlocking tightness through varying the macrocycle size, a feat traditionally inaccessible by non-interlocked analogues.
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Y. Zhang, H. T. Yau, Q. Chen, Y. Deng, Z. Ying, S. Lee, H. Y. Au-Yeung and E. C. M. Tse, Chem. Commun., 2026, Accepted Manuscript , DOI: 10.1039/D6CC02558G
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