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A sterically hindered organic Lewis acid catalyst B(C6F5)3 was utilized to regulate the reaction kinetics of COF-300 synthesis, enabling direct observation of the intermediate single-crystal growth stage. This approach establishes a novel experimental basis for mechanistic studies of COFs crystallization and provides valuable insight into controlled crystal formation pathways.
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T. Wang, M. Fu, H. Wang, C. Yi, D. Chen, Q. Liu, Y. Meng, J. Hu and T. Liu, Chem. Commun., 2026, Accepted Manuscript , DOI: 10.1039/D6CC02265K
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