An ice-templated CuPd/TiN catalyst is reported for efficient, basefree photocatalytic Glaser homocoupling. Synergizing TiN's LSPR effect with CuPd alloying, the system achieves 99% conversion and 100% selectivity. XAS-confirmed electron transfer from Cu to Pd facilitates superoxide radical generation, providing a robust and sustainable strategy for green C-C coupling.
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H. Hao, Y. Li, T. Han and Q. Xiao, Chem. Commun., 2026, Accepted Manuscript , DOI: 10.1039/D6CC01511E
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