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Flow NMR is indispensable in reaction monitoring, while diffusion NMR aids mixture analysis. Signal overlap remains a concern in 2D diffusion NMR. Distributing spectral information over two chemical-shift dimensions improves peak resolution and enables cross-correlations. We present a flow-compensated DOSY ultrafast COSY experiment acquiring a 3D dataset in 5 minutes.
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Y. Horbenko, P. Giraudeau, F. Felpin and J. Dumez, Chem. Commun., 2026, 62, 10763 DOI: 10.1039/D6CC01422D
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