We report an electrochemical alkene thiooxygenation using 2-hydroxy-1-ethanethiol and styryl azides to access oxathiazinane. This method generates sulfur radicals in situ without oxidants or catalysts, offering excellent regioselectivity and addressing a key challenge in heterocycle synthesis.
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Z. Lin, Z. Lei, X. Meng, W. Wang, H. Tang and Y. Pan, Chem. Commun., 2026, Accepted Manuscript , DOI: 10.1039/D6CC01416J
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