In this paper, an osmium catalyzed oxidative cyclization of 1,4-dienes is reported. The reaction undergoes exo,exo-type cyclization, with oxetanes obtained for the first time as oxidative cyclization products. Catalytic amount of potassium osmate dihydrate was used with sodium periodinate as a terminal oxidant.
S. Wang, Y. Zhang, C. Wang and L. Zong, Org. Biomol. Chem., 2025, Accepted Manuscript , DOI: 10.1039/D6OB00220J
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