A visible-light promoted sulfenylation of N-carboxyindoles with thiols showed substantially higher rate and selectivity when conducted “on water”. An EDA complex was proposed to form at the water–oil interface, generating thiyl radicals and thus initiating a chain reaction.
J. S. Lee, C. Lee, J. Jang and S. Shin, Org. Biomol. Chem., 2025, 23, 3325 DOI: 10.1039/D5OB00429B
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