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Abstract | Cited by

A 6-step gram-scale synthesis of the fungal polyketide (±)-gregatin A is described. The synthetic route features an intermolecular 1,3-dipolar cycloaddition, a Mo-mediated disconnection of the isoxazole skeleton, and an acid-mediated deprotection/enamine hydrolysis and hemiketalization cascade.

Graphical abstract: Scalable synthesis of (±)-gregatin A via a 1,3-dipolar cycloaddition strategy

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