A facile synthesis of multi(triazole)s by iterative click reactions is disclosed. Good functional group tolerance of sequential click assembly by sulfur–fluoride exchange (SuFEx), copper-catalyzed azide–alkyne cycloaddition (CuAAC), and thia-Michael reaction realizes the iterative click reactions. Diverse multi(triazole)-type mid-molecules can be synthesized easily from readily available modules through good chemoselective reactions without functional group transformation steps.
G. Orimoto and S. Yoshida, Chem. Commun., 2024, 60, 5824 DOI: 10.1039/D4CC01177E
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