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Abstract | Cited by

An efficient iron-catalyzed alkoxyl radical-mediated C–C bond cleavage/phosphorothiolation cascade is presented. This protocol features mild and redox neutral conditions, wide substrate scope and easy scalability, allowing straightforward access to functionalized S-alkyl organophosphorus compounds in moderate to good yields.

Graphical abstract: Iron-catalyzed alkoxyl radical-mediated C–C bond cleavage/phosphorothiolation: a new approach to functionalized S-alkyl phosphorothioates

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