A palladium-catalyzed disilylation reaction applicable for a variety of non-, α-, or β-substituted and α,β-disubstituted ortho-halophenylethylenes has been developed. This reaction proceeds with high yields and very low catalyst loadings. The two C–Si bonds of the disilylated products could be well-differentiated chemoselectively in the reaction with various electrophiles.
B. Zhu, S. Zhang, J. Fu, G. Lin and C. Feng, Chem. Commun., 2023, 59, 5922 DOI: 10.1039/D3CC01452E
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