Issue 5, 2022
From the journal:

Reaction Chemistry & Engineering

Mono- and sym-pentahalogenated corannulenes: reaction optimization & purification by in process product analysis†

Bokai Xu,‡a   Tianjian Guo‡a  and  Jay Siegel ORCID logo *a  

* Corresponding authors

a School of Pharmaceutical Science and Technology, Tianjin University, 92 Weijin Road, Tianjin, PR China
E-mail: siegeljsx@gmail.com

Abstract

A robust, mild & inexpensive synthetic route to mono-halogenated corannulene and a robust method for purifying and analyzing sym-pentachlorocorannulene from the ICl halogenation of corannulene is reported.

Graphical abstract: Mono- and sym-pentahalogenated corannulenes: reaction optimization & purification by in process product analysis

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Article information

DOI
https://doi.org/10.1039/D2RE00010E
Article type
Paper
Submitted
08 Jan 2022
Accepted
21 Feb 2022
First published
02 Mar 2022

React. Chem. Eng., 2022,7, 1230-1235

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Mono- and sym-pentahalogenated corannulenes: reaction optimization & purification by in process product analysis

B. Xu, T. Guo and J. Siegel, React. Chem. Eng., 2022, 7, 1230 DOI: 10.1039/D2RE00010E

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