Issue 36, 2022
From the journal:

Chemical Communications

SHARPER-enhanced benchtop NMR: improving SNR by removing couplings and approaching natural linewidths†

Claire L. Dickson, ORCID logo a   George Peat,a   Matheus Rossetto,b   Meghan E. Halse ORCID logo b  and  Dušan Uhrín ORCID logo *a  

* Corresponding authors

a EaStCHEM School of Chemistry, University of Edinburgh, Edinburgh, UK
E-mail: dusan.uhrin@ed.ac.uk

b Department of Chemistry, University of York, York, UK

Abstract

We present a signal enhancement strategy for benchtop NMR that produces SNR increases on the order of 10 to 30 fold by collapsing the target resonance into an extremely narrow singlet. Importantly, the resultant signal is amenable to quantitative interpretation and therefore can be applied to analytical applications such as reaction monitoring.

Graphical abstract: SHARPER-enhanced benchtop NMR: improving SNR by removing couplings and approaching natural linewidths

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Article information

DOI
https://doi.org/10.1039/D2CC01325H
Article type
Communication
Submitted
06 Mar 2022
Accepted
04 Apr 2022
First published
05 Apr 2022
This article is Open Access
Creative Commons BY license

Chem. Commun., 2022,58, 5534-5537

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SHARPER-enhanced benchtop NMR: improving SNR by removing couplings and approaching natural linewidths

C. L. Dickson, G. Peat, M. Rossetto, M. E. Halse and D. Uhrín, Chem. Commun., 2022, 58, 5534 DOI: 10.1039/D2CC01325H

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