Issue 67, 2021
From the journal:

Chemical Communications

Sulfonyl radical triggered selective iodosulfonylation and bicyclization of 1,6-dienes†

Shi-Ping Wu,a   Dong-Kai Wang,a   Qing-Qing Kang,a   Guo-Ping Ge,a   Hongxing Zheng,b   Meiling Zhu,c   Ting Li, ORCID logo *c   Jun-Qi Zhangd  and  Wen-Ting Wei ORCID logo *a  

* Corresponding authors

a Key Laboratory of Advanced Mass Spectrometry and Molecular Analysis of Zhejiang Province, State Key Laboratory for Managing Biotic and Chemical Threats to the Quality and Safety of Agro-Products, School of Materials Science and Chemical Engineering, Ningbo University, Ningbo, Zhejiang, China
E-mail: weiwenting@nbu.edu.cn

b Institution of Functional Organic Molecules and Materials, School of Chemistry and Chemical Engineering, Liaocheng University, Liaocheng, Shandong, China

c College of Chemistry and Pharmaceutical Engineering, Nanyang Normal University, Nanyang, Henan, China

d Advanced Research Institute and Department of Chemistry, Taizhou University, 1139 Shifu Avenue, Taizhou, China

Abstract

A novel sulfonyl radical triggered selective iodosulfonylation and bicyclization of 1,6-dienes has been described for the first time. High selectivity and efficiency, mild reaction conditions, excellent functional group compatibility, and broad substrate scope are the attractive features of this synthetic protocol, which provides a unique platform for precise radical cyclization.

Graphical abstract: Sulfonyl radical triggered selective iodosulfonylation and bicyclization of 1,6-dienes

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Article information

DOI
https://doi.org/10.1039/D1CC03252F
Article type
Communication
Submitted
19 Jun 2021
Accepted
14 Jul 2021
First published
15 Jul 2021

Chem. Commun., 2021,57, 8288-8291

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Sulfonyl radical triggered selective iodosulfonylation and bicyclization of 1,6-dienes

S. Wu, D. Wang, Q. Kang, G. Ge, H. Zheng, M. Zhu, T. Li, J. Zhang and W. Wei, Chem. Commun., 2021, 57, 8288 DOI: 10.1039/D1CC03252F

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