Pd-catalyzed allylic C–H activation of simple olefins allows an easy entry to seven-membered N,O-heterocycles such as 1,4-benzoxazepines (1,4-BZOs), 1,4-benzodiazepinones (1,4-BZDs) and 1,4-oxazepanes in good to excellent yields. Straightforward derivatization of the olefinated 1,4-BZO shows the synthetic utility of this methodology.
Á. Velasco-Rubio, J. A. Varela and C. Saá, Chem. Commun., 2021, 57, 10915 DOI: 10.1039/D1CC04056A
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