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Synthesis and chemical stability of technetium nitrides

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Abstract

We demonstrate the synthesis and phase stability of TcN, Tc2N, and a substoichiometric TcNx from 0 to 50 GPa and to 2500 K in a laser-heated diamond anvil cell. At least potential recoverability is demonstrated for each compound. TcN adopts a previously unpredicted structure identified via crystal structure prediction.

Graphical abstract: Synthesis and chemical stability of technetium nitrides

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Article information


Submitted
12 May 2021
Accepted
11 Jul 2021
First published
12 Jul 2021

Chem. Commun., 2021, Advance Article
Article type
Communication

Synthesis and chemical stability of technetium nitrides

E. Siska, D. Smith, A. Salamat, K. V. Lawler, B. Lavina, F. Poineau and P. M. Forster, Chem. Commun., 2021, Advance Article , DOI: 10.1039/D1CC02525B

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