Understanding of TEMPO-electrocatalyzed acceptorless dehydrogenation of tetrahydroquinoline by in situ extractive electrospray ionization mass spectrometry

Weixiang Li; Jianghui Sun; Yan Wang; Jinping Qiao; Lixin He; Jin Ouyang; Na Na

doi:10.1039/D0CC08209K

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Understanding of TEMPO-electrocatalyzed acceptorless dehydrogenation of tetrahydroquinoline by in situ extractive electrospray ionization mass spectrometry†

Weixiang Li,^a Jianghui Sun,^a Yan Wang,

^a Jinping Qiao,^a Lixin He,^a Jin Ouyang

^a and Na Na

*^a

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* Corresponding authors

^a Key Laboratory of Radiopharmaceuticals, Ministry of Education, College of Chemistry, Beijing Normal University, Beijing 100875, China
E-mail: nana@bnu.edu.cn

Abstract

The TEMPO-electrocatalyzed acceptorless dehydrogenation of tetrahydroquinoline, a transformation in green synthesis and hydrogen storage, has been investigated by coupling of an electrocatalytic system with in situ extraction electrospray ionization mass spectrometry. Dynamic changes in important species and intermediates were monitored, which evoked an updated AD understanding.

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Article information

DOI: https://doi.org/10.1039/D0CC08209K
Article type: Communication
Submitted: 18 Dec 2020
Accepted: 08 Feb 2021
First published: 09 Feb 2021

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Chem. Commun., 2021,57, 2955-2958

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Understanding of TEMPO-electrocatalyzed acceptorless dehydrogenation of tetrahydroquinoline by in situ extractive electrospray ionization mass spectrometry

W. Li, J. Sun, Y. Wang, J. Qiao, L. He, J. Ouyang and N. Na, Chem. Commun., 2021, 57, 2955 DOI: 10.1039/D0CC08209K

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Chemical Communications

Understanding of TEMPO-electrocatalyzed acceptorless dehydrogenation of tetrahydroquinoline by in situ extractive electrospray ionization mass spectrometry†

Abstract

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Understanding of TEMPO-electrocatalyzed acceptorless dehydrogenation of tetrahydroquinoline by in situ extractive electrospray ionization mass spectrometry

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