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An entirely solvent-free photooxygenation of olefins under continuous flow conditions

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Abstract

Photooxygenations of alkenes with singlet oxygen are a versatile, atom-economical transformation. The choice of solvents is key to the success of this oxyfunctionalization with direct impact on the solubility of substrates, the lifetime of the reactive oxygen species, and the up-scaling of the process. We report an entirely solvent-free continuous-flow photooxygenation that operates at very high substrate/sensitizer ratios and enables high space–time yields.

Graphical abstract: An entirely solvent-free photooxygenation of olefins under continuous flow conditions

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Article information


Submitted
04 Feb 2020
Accepted
25 Mar 2020
First published
25 Mar 2020

Green Chem., 2020, Advance Article
Article type
Communication

An entirely solvent-free photooxygenation of olefins under continuous flow conditions

P. Bayer and A. Jacobi von Wangelin, Green Chem., 2020, Advance Article , DOI: 10.1039/D0GC00436G

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