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A general protocol for the synthesis of Pt-NHC (NHC = N-heterocyclic carbene) hydrosilylation catalysts

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Abstract

A general, user-friendly synthetic route to [Pt(NHC)(L)Cl2] and [Pt(NHC)(dvtms)] (L = DMS, Py; DMS = dimethyl sulfide, dvtms = divinyltetramethylsiloxane, Py = pyridine) complexes has been developed. The procedure is applicable to a wide range of ligands and enables facile synthetic access to key Pt(0)- and Pt(II)-NHC complexes used in hydrosilylation catalysis.

Graphical abstract: A general protocol for the synthesis of Pt-NHC (NHC = N-heterocyclic carbene) hydrosilylation catalysts

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Supplementary files

Article information


Submitted
11 Aug 2020
Accepted
09 Oct 2020
First published
09 Oct 2020

Dalton Trans., 2020, Advance Article
Article type
Paper

A general protocol for the synthesis of Pt-NHC (NHC = N-heterocyclic carbene) hydrosilylation catalysts

B. P. Maliszewski, N. V. Tzouras, S. G. Guillet, M. Saab, M. Beliš, K. Van Hecke, F. Nahra and S. P. Nolan, Dalton Trans., 2020, Advance Article , DOI: 10.1039/D0DT03480K

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