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Probing sulphur clusters in a microfluidic electrochemical cell with synchrotron-based photoionization mass spectrometry

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Abstract

We present synchrotron-based mass spectrometry to probe products formed in a lithium sulphide electrolyte. In operando analysis was carried out at two different potentials in a vacuum compatible microfluidic electrochemical cell. Mass spectral observations show that the charged electrolyte formed sulphur clusters under dynamic conditions, demonstrating electrolyte electron shuttling.

Graphical abstract: Probing sulphur clusters in a microfluidic electrochemical cell with synchrotron-based photoionization mass spectrometry

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Article information


Submitted
07 May 2020
Accepted
19 Jun 2020
First published
19 Jun 2020

Phys. Chem. Chem. Phys., 2020, Advance Article
Article type
Communication

Probing sulphur clusters in a microfluidic electrochemical cell with synchrotron-based photoionization mass spectrometry

R. Komorek, B. Xu, J. Yao, O. Kostko, M. Ahmed and X. Yu, Phys. Chem. Chem. Phys., 2020, Advance Article , DOI: 10.1039/D0CP02472D

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