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Atom economical coupling of benzophenone and N-heterocyclic aromatics with SmI2

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Abstract

The use of stoechiometric SmI2 in combination with benzophenone and N-heterocyclic aromatics such as bipyridine, phenanthroline and pyridine allows the direct ortho-coupling of both partners in an atom economical reaction free of any other coupling additives. The transformation was investigated by 1H NMR, X-ray studies and theoretical calculations providing reaction intermediates and the reaction mechanism.

Graphical abstract: Atom economical coupling of benzophenone and N-heterocyclic aromatics with SmI2

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Article information


Submitted
29 Jul 2020
Accepted
28 Aug 2020
First published
28 Aug 2020

Chem. Commun., 2020, Advance Article
Article type
Communication

Atom economical coupling of benzophenone and N-heterocyclic aromatics with SmI2

A. Jaoul, Y. Yang, N. Casaretto, C. Clavaguéra, L. Maron and G. Nocton, Chem. Commun., 2020, Advance Article , DOI: 10.1039/D0CC05164K

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