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Monitoring polymer-assisted mechanochemical cocrystallisation through in situ X-ray powder diffraction

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Abstract

Time-resolved mechanochemical cocrystallisation studies have so-far focused solely on neat and liquid-assisted grinding. Here, we report the investigation of polymer-assisted grinding reactions using in situ X-ray powder diffraction, revealing that reaction rate is almost double compared to neat grinding and independent of the molecular weight and amount of the polymer additive used.

Graphical abstract: Monitoring polymer-assisted mechanochemical cocrystallisation through in situ X-ray powder diffraction

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Article information


Submitted
14 May 2020
Accepted
22 Jun 2020
First published
22 Jun 2020

Chem. Commun., 2020, Advance Article
Article type
Communication

Monitoring polymer-assisted mechanochemical cocrystallisation through in situ X-ray powder diffraction

L. S. Germann, S. T. Emmerling, M. Wilke, R. E. Dinnebier, M. Moneghini and D. Hasa, Chem. Commun., 2020, Advance Article , DOI: 10.1039/D0CC03460F

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