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[3+1+1] type cyclization of ClCF2COONa for the assembly of imidazoles and tetrazoles via in situ generated isocyanides

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Abstract

A facile synthesis of imidazoles and tetrazoles via [3+1+1] type cyclization of ClCF2COONa is developed. A diverse array of imidazoles and tetrazoles were obtained in decent yields via isocyanide intermediates. Notably, this is the first example of the cycloaddition of in situ generated isocyanides.

Graphical abstract: [3+1+1] type cyclization of ClCF2COONa for the assembly of imidazoles and tetrazoles via in situ generated isocyanides

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Article information


Submitted
13 Mar 2020
Accepted
20 Apr 2020
First published
20 Apr 2020

Chem. Commun., 2020, Advance Article
Article type
Communication

[3+1+1] type cyclization of ClCF2COONa for the assembly of imidazoles and tetrazoles via in situ generated isocyanides

Y. Wang, Y. Zhou and Q. Song, Chem. Commun., 2020, Advance Article , DOI: 10.1039/D0CC01919D

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