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Black phosphorus as a metal-free, visible-light-active heterogeneous photoredox catalyst for the direct C–H arylation of heteroarenes

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Abstract

Black phosphorus (BP) is for the first time employed as a metal-free, heterogeneous photoredox catalyst for the direct C–H arylation of heteroarenes with aryl diazonium salts. The arylated heteroarenes are obtained in moderate to good yields under visible-light illumination, and the protocol is shown to be applicable for the scale-up synthesis.

Graphical abstract: Black phosphorus as a metal-free, visible-light-active heterogeneous photoredox catalyst for the direct C–H arylation of heteroarenes

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Article information


Submitted
11 Mar 2020
Accepted
17 Apr 2020
First published
17 Apr 2020

Chem. Commun., 2020, Advance Article
Article type
Communication

Black phosphorus as a metal-free, visible-light-active heterogeneous photoredox catalyst for the direct C–H arylation of heteroarenes

E. Kalay, H. Küçükkeçeci, H. Kilic and Ö. Metin, Chem. Commun., 2020, Advance Article , DOI: 10.1039/D0CC01874K

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