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Electrochemical nickel-catalyzed Migita cross-coupling of 1-thiosugars with aryl, alkenyl and alkynyl bromides

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Abstract

Here we report a simple route towards the synthesis of thioglycosides, in which electrochemical cross-coupling is used to form a S–C glycosidic bond from protected and unprotected thiosugars with functionalized aryl bromides under base free conditions. The reaction manifold that we report here demonstrates the power of electrochemistry to access highly complex glycosides under mild conditions.

Graphical abstract: Electrochemical nickel-catalyzed Migita cross-coupling of 1-thiosugars with aryl, alkenyl and alkynyl bromides

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Submitted
12 Feb 2020
Accepted
10 Mar 2020
First published
10 Mar 2020

Chem. Commun., 2020, Advance Article
Article type
Communication

Electrochemical nickel-catalyzed Migita cross-coupling of 1-thiosugars with aryl, alkenyl and alkynyl bromides

M. Zhu, M. Alami and S. Messaoudi, Chem. Commun., 2020, Advance Article , DOI: 10.1039/D0CC01126F

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