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Selective synthesis of azoxybenzenes from nitrobenzenes by visible light irradiation under continuous flow conditions

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Abstract

Herein, we report a highly selective preparation method of azoxybenzenes from nitrobenzenes by visible-light irradiation. In a batch, this reaction method affords the corresponding aniline derivatives or intermediates (nitrosobenzene or phenyl hydroxylamine); however, in flow microreactors, azoxybenzenes are successfully obtained with very high selectivity.

Graphical abstract: Selective synthesis of azoxybenzenes from nitrobenzenes by visible light irradiation under continuous flow conditions

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Publication details

The article was received on 05 Jul 2019, accepted on 05 Aug 2019 and first published on 05 Aug 2019


Article type: Communication
DOI: 10.1039/C9RE00265K
React. Chem. Eng., 2019, Advance Article

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    Selective synthesis of azoxybenzenes from nitrobenzenes by visible light irradiation under continuous flow conditions

    Y. Nishiyama, A. Fujii and H. Mori, React. Chem. Eng., 2019, Advance Article , DOI: 10.1039/C9RE00265K

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