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Synthesis of photolabile protecting group (PPG) protected uronic acid building blocks: applications in carbohydrate synthesis with the assistance of a continuous flow photoreactor

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Abstract

Photolabile protecting group (PPG) protected uronic acid building blocks were prepared and used for carbohydrate synthesis. Deprotection of the photolabile protecting group was achieved very efficiently by employing a continuous flow photoreactor under neutral conditions. Many conventional protecting groups were found to be stable during the photo-cleavage of the 2-nitrobenzyl group at 355 nm in methanol.

Graphical abstract: Synthesis of photolabile protecting group (PPG) protected uronic acid building blocks: applications in carbohydrate synthesis with the assistance of a continuous flow photoreactor

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Publication details

The article was received on 13 Aug 2019, accepted on 13 Oct 2019 and first published on 14 Oct 2019


Article type: Research Article
DOI: 10.1039/C9QO01010F
Org. Chem. Front., 2019, Advance Article

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    Synthesis of photolabile protecting group (PPG) protected uronic acid building blocks: applications in carbohydrate synthesis with the assistance of a continuous flow photoreactor

    V. Tiwari, A. K. Singh, P. Chaudhary, P. H. Seeberger and J. Kandasamy, Org. Chem. Front., 2019, Advance Article , DOI: 10.1039/C9QO01010F

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