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Exploring wet chemistry approaches to ZnFe2O4 spinel ferrite nanoparticles with different inversion degrees: a comparative study

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Abstract

Zinc ferrite (ZnFe2O4) spinel nanocrystals were synthesised through three different low-temperature routes, namely hydrothermal, combined miniemulsion/hydrothermal, and microwave-assisted non-aqueous sol–gel synthesis. With the aim of studying the influence of the respective approach on the structural evolution of the compounds during the synthetic process, the samples were prepared with different processing times. The resulting nanoparticles were inspected with a wide range of analytical techniques, both with regards to the local (X-ray absorption spectroscopy – XAS) and the long-range (Raman spectroscopy, X-ray diffraction – XRD) order.

Graphical abstract: Exploring wet chemistry approaches to ZnFe2O4 spinel ferrite nanoparticles with different inversion degrees: a comparative study

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Publication details

The article was received on 06 Mar 2019, accepted on 02 May 2019 and first published on 06 May 2019


Article type: Research Article
DOI: 10.1039/C9QI00241C
Inorg. Chem. Front., 2019, Advance Article

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    Exploring wet chemistry approaches to ZnFe2O4 spinel ferrite nanoparticles with different inversion degrees: a comparative study

    P. Dolcet, K. Kirchberg, A. Antonello, C. Suchomski, R. Marschall, S. Diodati, R. Muñoz-Espí, K. Landfester and S. Gross, Inorg. Chem. Front., 2019, Advance Article , DOI: 10.1039/C9QI00241C

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